中国半导体行业协会封装分会会刊

中国电子学会电子制造与封装技术分会会刊

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电子与封装 ›› 2021, Vol. 21 ›› Issue (8): 080405 . doi: 10.16257/j.cnki.1681-1070.2021.0815

• 微电子制造与可靠性 • 上一篇    下一篇

低压化学气相淀积低应力氮化硅工艺研究

王敬轩;商庆杰;杨志   

  1. 中国电子科技集团公司第十三研究所,石家庄 050000
  • 收稿日期:2020-02-09 出版日期:2021-08-11 发布日期:2021-04-28
  • 作者简介:王敬轩(1988—),男,河北石家庄人,硕士,工程师,现从事微电子制造工艺研究。

Research on LowStress Silicon Nitride by Using Low Pressure Chemical-Vapor Deposition Process

WANG Jingxuan, SHANG Qingjie, YANG Zhi   

  1. China Electronics Technology GroupCorporation No.13 Research Institute,
  • Received:2020-02-09 Online:2021-08-11 Published:2021-04-28

摘要: 微机械加工(MEMS)工艺中常需要应用到低应力氮化硅作为结构层或钝化层材料,以降低圆片的翘曲。通过采用低压化学气相淀积工艺(LPCVD),优化工艺中反应气体流量比,可以得到应力低于200 MPa的氮化硅薄膜。针对工艺中存在的片间应力以及薄膜厚度均匀性差的问题,采用二次电子质谱(SIMS)的方式,分析出反应气体的消耗造成的反应气体比例变化是引起该问题的主要因素。通过优化工艺参数,得到了片间应力在100~150 MPa之间、厚度均匀性5%以内的低应力氮化硅薄膜,可实现50片/炉的工艺能力,可批量应用于微机械加工(MEMS)工艺中。

关键词: 微机械加工, 低压化学气相淀积, 低应力氮化硅, 均匀性

Abstract: In order to flatten the bow of wafers, low stress silicon nitride is often used in the micro-electro mechanical system as structural layer materials or passivation films. We can obtain the silicon nitride films whose stress are under 200 MPa pascal through optimizing the ratio of the reaction gases in low pressure chemical-vapor deposition. Bad wafer to wafer non-uniformity of films’ stress and thickness is an important process problem. We analyzed that the change of ratio caused by the consumption of the reaction gases is the main factor in the method of using secondary ion mass spectroscopy (SIMS). By optimizing the process parameters, we can obtain the silicon nitride films whose wafer to wafer stress is between 100 to 150 MPa Pascal and thickness non-uniformity is below 5%. And we can also realize the process capability of 50 wafers per furnace, which can be used in micro-electro mechanical system process in the future.

Key words: micro-electromechanicalsystem, lowpressurechemical-vapordeposition, lowstresssiliconnitride, un-uniformity

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